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Post-synthetic and in situ engineering of metal nanoclusters for enhanced stability and multifunctional applications

Anal. Methods, 2026, Advance Article
DOI: 10.1039/D6AY00154H, Critical Review

Ritika Mittal, Nancy Gupta
Engineering metal nanoclusters via post-synthetic and in situ strategies enhances stability and photoluminescence while enabling new functionalities. This review critically evaluates these approaches, associated properties, and applications.
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A highly sensitive SERS sensor for malachite green detection based on spiky Fe3O4@Au supraparticles

Anal. Methods, 2026, Advance Article
DOI: 10.1039/D6AY00166A, Paper

Hang Ye, Yanke Wang, Hufu Chen, Tao Huang, Shengnan Zhan
A novel label-free analytical strategy based on surface-enhanced Raman spectroscopy (SERS) has been developed for the detection of malachite green (MG) using spiky Fe₃O₄@Au supraparticles (Fe₃O₄@AuSPs).
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Correction: Rapid point-of-care detection of vitamin D deficiency using disposable electrochemical immunosensors based on a La2O3-WO3@CNT Bi-metal oxide nanocomposite

Anal. Methods, 2026, 18,3239-3239
DOI: 10.1039/D6AY90044E, Correction

Open Access

&nbsp This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.

Omar Ramadan, Mostafa Ahmed, Pradeep Kumar Brahman, Daohong Zhang, Rabeay Y. A. Hassan
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Rational design of environment-sensitive fluorescent probes for butyrylcholinesterase and their application in biological imaging

Anal. Methods, 2026, 18,3216-3223
DOI: 10.1039/D6AY00158K, Paper

Lulian Shao, Feng Wang, Yu Wang, Jiahao Du, Wenting Cao, Qingwen Zhang, Fenqin Zhao, Junfeng Wang, Wenhui Fan, Yuemin Zhou, Bingxin Wang, Xiaobin Pang, Lin Yan
Rational design of environment-sensitive fluorescent probes for butyrylcholinesterase and their application in biological imaging.
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Green analytical approach for multielemental determination in oily matrices combining extraction induced by emulsion breaking (EIEB) with ICP OES

Anal. Methods, 2026, 18,3184-3197
DOI: 10.1039/D6AY00110F, Paper

Maria Isadora Pereira Lima, Lucas Rafael de Moura Domingos, Naomi Akiba, Ivanise Gaubeur
Extraction induced by emulsion breaking: a low-impact, solvent-saving analytical method for oil sample preparation and multielement metal determination by emulsion techniques.
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Development of an effective preconcentration strategy for the trace determination of nickel in thyme tea extracts by FeSbO4 nanoparticle-based dispersive solid phase extraction (DSPE)

Anal. Methods, 2026, 18,3163-3171
DOI: 10.1039/D5AY02102B, Paper

Open Access

&nbsp This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.

Muhammed Ali Büyük, Hakan Serbest, Sezgin Bakırdere
FeSbO₄ nanoparticles were fabricated under hydrothermal synthesis conditions and utilized for the first time as sorbent materials for the preconcentration/separation of Ni ions.
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A unified UPLC-MS/MS method for simultaneous quantification of intact anthocyanins and their metabolites in rat plasma

Anal. Methods, 2026, 18,3153-3162
DOI: 10.1039/D6AY00186F, Paper

Chunzi Zhang, Guzhalinuer Aierken, Xiaoyan Ma, Tuxia Pang, Juan Zhang, Mihriban Arken, Shuyong Yu, Qianghui Mian, Xiaoli Ma
This study developed and validated a rapid UPLC-MS/MS method for the simultaneous determination of anthocyanins and their metabolites in rat plasma.
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DNA-mediated synergistic proximity ligation for ultrasensitive electrochemiluminescence detection of microcystin-LR

Anal. Methods, 2026, 18,3065-3073
DOI: 10.1039/D6AY00161K, Paper

Hongfang Gao, Rong Xiao, Taotao Ma, Xiaolin Yang, Shangxian Ma
An innovative ECL aptasensor based on a DNA-mediated synergistic proximity cooperative complex comprising three ferrocene groups was developed for MC-LR detection.
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A TiO2/Ti3C2 MXene photoelectrochemical chip with multiphysics field engineering for quantification of wastewater DNA

Anal. Methods, 2026, 18,3098-3111
DOI: 10.1039/D6AY00099A, Paper

Qitong Zeng, Xiaojie Ma, Tianci Liu, Zedong Liang, Shengxin Liu, Shuohua Zhang, Changbiao Chi
This study develops a TiO₂/Ti₃C₂ MXene heterojunction-based photoelectrochemical microfluidic chip enhanced by acoustic and magnetic multiphysics fields for ultrasensitive detection of wastewater DNA.
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Rapid point-of-care detection of vitamin D deficiency using disposable electrochemical immunosensors based on a La2O3-WO3@CNT Bi-metal oxide nanocomposite

Anal. Methods, 2026, 18,3086-3097
DOI: 10.1039/D6AY00076B, Paper

Omar Ramadan, Mostafa Ahmed, Pradeep Kumar Brahmana, Daohong Zhang, Rabeay Y. A. Hassan
The nanostructured sensing system is designed and fully optimized with vitamin D-specific biorecognition probes, then integrated onto a disposable substrate to fabricate a portable device for vitamin D level testing.
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