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Preparation of MIL-68@Fe3O4@PVDF composites via the spray phase inversion method and their magnetic solid-phase extraction of parabens and bisphenol A

Anal. Methods, 2026, Advance Article
DOI: 10.1039/D6AY00276E, Paper

Xinwen Hu, Yong Zhang, Zhihao Chen, Mengqian Xiao, Litao Wang, Guihua Gao
MIL-68@Fe₃O₄@PVDF composites were prepared by the spray phase inversion method and used for MSPE of parabens and BPA.
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Development and validation of a QbD-integrated sensitive RP-HPLC method for quantitation of fenofibrate: an application in quality control

Anal. Methods, 2026, Advance Article
DOI: 10.1039/D5AY01843A, Paper

Romi Singh, Abhiram Kumar, Ashutosh Pareek, Dipti Srivastava, Madhaw Kumar, Mohini Chaurasia, S. J. S. Flora
The present study aims to develop and validate a robust, sensitive HPLC method for the estimation of fenofibrate in a gel-matrix sustained-release tablet formulation designed to prevent alcohol-induced dose dumping.
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A ratiometric fluorescence/colorimetric dual-response sensor based on fluorescent nanozymes and smartphone-assisted readout for the accurate determination of glyphosate residues

Anal. Methods, 2026, Advance Article
DOI: 10.1039/D6AY00379F, Paper

Xuhai Ding, Ying Zhang, Tao Bo, Jinhua Zhang, Wenyan Yan, Baoqing Bai, Yukun Yang
A Cu-BH MOF nanozyme-based fluorescence/colorimetric dual-response sensor for visual glyphosate detection with ultra-low limits via smartphone RGB readout.
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Unsupervised and supervised methodologies for identification of sample pixels in Fourier transform infrared microspectroscopic images

Anal. Methods, 2026, Advance Article
DOI: 10.1039/D5AY02095F, Paper

Xiangyu Zhao, Yudong Tian, Jingzhu Shao, Chongzhao Wu
A framework combining unsupervised and supervised methods is presented for sample pixel identification in FTIR microspectroscopy. This integrated solution ensures accurate detection and streamlines FTIR signal processing for further applications.
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Construction of a highly sensitive electrochemical sensing platform using an Au-RGO-MWCNTs nanocomposite for the synergistic amplification of rutin detection

Anal. Methods, 2026, Accepted Manuscript
DOI: 10.1039/D6AY00661B, Paper

Ling-Zhi He, Xiang Li, Zhi-Wen Zeng, Yang Hong, Chi-Qiong Liu, Zhong-Hou Liang, WenAn Kuang
Rutin, a naturally occurring bioactive flavonoid glycoside, has considerable medicinal importance, making its accurate and rapid detection of great significance. Herein, we report a highly sensitive electrochemical sensor for the...
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Selection and characterization of DNA aptamers specific to trichlorfon

Anal. Methods, 2026, Accepted Manuscript
DOI: 10.1039/D6AY00588H, Paper

Shuting Yang, Dan Wei, Ziyu He, Li Li, Tong Zhou, Xueying Liu, Yan Deng
In this study, six candidate DNA aptamers specific to trichlorfon were successfully obtained through 16 rounds of capture-SELEX. Their binding affinity were rigorously evaluated and comparatively analyzed using three orthogonal...
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Quartz crystal microbalance determination of acephate based on molecularly imprinting polymer and sulphur doped copper ferrites

Anal. Methods, 2026, Accepted Manuscript
DOI: 10.1039/D6AY00590J, Paper

Open Access

&nbsp This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence.

Bahar Bankoğlu BANKOĞLU
Acephate (ACE), an effective systemic insecticide, plays a significant role in agricultural pest control. For many decades, this compound can be used to manage various insect infestations in the crops,...
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A green analytical assay for the quantitation of bioavailable phosphorus in soils: in situ extraction and smartphone-based measurement

Anal. Methods, 2026, Advance Article
DOI: 10.1039/D6AY00101G, Paper

Stella Sales Macedo, Edilene Cristina Ferreira, Arnaldo Alves Cardoso
A sustainable method for quantifying bioavailable phosphorus in soils using ultrasound-assisted extraction and smartphone-based digital image colorimetry, enabling rapid and portable analysis.
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Advanced GC Method for Comprehensive Residual Solvent Analysis: Overcoming Co-elution with Orthogonal Columns and Quantification by Mass Spectrometry

Anal. Methods, 2026, Accepted Manuscript
DOI: 10.1039/D5AY01603G, Paper

Ruba A Arulraj, VINAY VISHWANATH, Sharad Duche, Arvind Mathur, Amrita Roy Roy
A robust and comprehensive gas chromatographic method was developed to identify and quantify the 57 residual solvents listed in the ICH guidelines, all in a single, 30-minute chromatogram. The proposed...
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Analytical workflows in salivary metabolomics for athlete stress monitoring: sampling, platform selection, and translation challenges

Anal. Methods, 2026, Accepted Manuscript
DOI: 10.1039/D6AY00755D, Minireview

Fei Liu, Xiaotian Gao, Xiaoping Wang, Song Yuan, Chan Wang
Salivary metabolomics has emerged as a promising non-invasive strategy for athlete stress monitoring, but its translational value depends as much on analytical rigor as on biomarker discovery. This review examines...
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